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Laboratory Manual in Engineering Chemistry : For the Students of JNTU Hyderabad

Laboratory Manual in Engineering Chemistry : For the Students of JNTU Hyderabad

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  • ISBN : 9789355016232
  • Pages : 136
  • Binding : Paperback
  • Language : English
  • Imprint : S. Chand Publishing
  • © year : 2023
  • Size : 6.5"X9.25

Price : 125.00 92.50

  • Dr. B. Rama Devi: Prof & Head Department of Chemistry, Board of Studies Chairman, JNTU Hyderabad
  • Dr. P. Aparna: Assistant Professor, Department of Chemistry, JNTU Hyderabad

The book is written to gain the basic knowledge on the principles of chemistry required for practical applications in engineering concepts. This book consists organic and general chemistry experiments for chemical engineering for 1st and 2nd semester students. The book also explains the precautions and safety rules for avoiding the accidents in chemistry laboratory. It covers Estimation of Ferrous iron by Dichrometry and Permanganometry Method, Estimation of Acetic Acid by Conductometric Titrations, Estimation of the Amount of Fe+2 by Potentiomentry, Determination of an Acid Concentration using pH Meter, Preparation of Nylon-6 and Bakelite (Phenol-Formaldehyde Resin), Estimation of Acid Value of Given Lubricant Oil, Determination of Rate of Corrosion of Mild Steel, Preparation of Benzanilide from Benzophenone via the Oxime by Beckmann Rearrangement etc.

I. VOLUMETRIC ANALYSIS

  1. Estimation of Ferrous iron by Dichrometry Method
  2. Estimation of Ferrous iron by Permanganometry Method
  3. Determination Estimation of Hardness of water by Complexometry Method Using EDTA
II. CONDUCTOMETRY
  1. Estimation of the Strength of an Acid by Conductometry
  2. Estimation of Acetic Acid by Conductometric Titrations
III. POTENTIOMETRY
  1. Estimation of the Amount of Fe+2 by Potentiomentry
IV. pH METRY
  1. Determination of an Acid Concentration using pH Meter
V. PREPARATIONS
  1. Preparation of Bakelite (Phenol-Formaldehyde Resin)
  2. Preparation of Nylon-6
VI. LUBRICANTS
  1. Estimation of Acid Value of Given Lubricant Oil
  2. Determination of Saponification Value of a Lubricant Oil
  3. Determination of Viscosity of Lubricant Oil Using Ostwald's Viscometer
VII. CORROSION
  1. Determination of Rate of Corrosion of Mild Steel
  2. Determination of Rate of Corrosion of Mild Steel in the Presence and Absence of Inhibitor
VIII. ORGANIC PREPRATION
  1. Preparation pf m-Dinitrobenzene from Nitrobenzene by Nitration
  2. Preparation of Benzanilide from Benzophenone via the Oxime by Beckmann Rearrangement
  3. Preparation of Benzylideneacetophenone from Benzaldehyde & Acetophenone by Claisen-Schmidt Reaction
  4. Cycloaddition of Anthracene with Maleic Anhydride by Diels-Alder Reaction
  5. Preparation of Benzoic Acid and Benzyl Alcohol from Benzaldehyde using Canizzaro's Reaction
  6. Preparation of β-Napthylbenzoate Using α-Napthol and Benzoyl Chloride using Schotten-Baumann Reaction
  7. Preparation of Acetylsalicylic Acid (Aspirin) from Salicylic Acid
  8. Preparation of Hippuric Acid from Glycine and Benzoyl Chloride
  9. Preparation of 7-Hydroxy-4-Methylcoumarin Using Resorcinol and Ethyl Acetoacetate
  10. Preparation of Azalactone from Hippuric Acid
  11. Preparation of Tribromo Aniline from Aniline
  12. Preparation of Tribromophenol from Phenol

Qualitative Organic Analysis
Physical Chemistry Experiments


 

  • The basic aim of the book is to inculcate the ability to design an experiment, to make observations carefully and to draw the conclusions out of experimental data.
  • This book is divided in 8 parts and all parts consist of relevant experiments.
  • Student's requirements are given top priority and the material is fashioned in a student-friendly style.

This book has been written as per the Common syllabus for B.Tech 1st and 2nd Semester students pursuing their B.Tech degree course in JNT University Hyderabad, Hyderabad.

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